HCID 19921378, compound → HCID 19921204, compound

HRID 1647885Notes

Reaction equation

HRID 1647885 reaction equation
Cl.[C:2]([C:5]1[CH:10]=[CH:9][C:8]([C:11]2[N:15]([CH2:16][CH2:17][CH2:18][C:19]([O:21]C)=[O:20])[C:14]3[CH:23]=[CH:24][C:25]([C:27]([NH:29][CH2:30][CH2:31][C:32]([O:34][CH3:35])=[O:33])=[O:28])=[CH:26][C:13]=3[N:12]=2)=[CH:7][CH:6]=1)(=[NH:4])[NH2:3]>C(Cl)Cl.CO>[C:2]([C:5]1[CH:10]=[CH:9][C:8]([C:11]2[N:15]([CH2:16][CH2:17][CH2:18][C:19]([OH:21])=[O:20])[C:14]3[CH:23]=[CH:24][C:25]([C:27]([NH:29][CH2:30][CH2:31][C:32]([O:34][CH3:35])=[O:33])=[O:28])=[CH:26][C:13]=3[N:12]=2)=[CH:7][CH:6]=1)(=[NH:3])[NH2:4]

Participants

3

Reactant 1

HCID 19921378HCID 19921378, compound

Product 1

HCID 19921204HCID 19921204, compound

Reagents, catalysts & solvents 1

HCID 21226129Dichloromethane methanolSolvent

Procedure

Obtained as a by-product in (120) Rf value: 0.19 (silica gel; methylene chloride/methanol=8:2)

Sources & evidence

ORD record
ord-fef771a2af124cb8a9989508749aea2c
Source dataset
uspto-grants-1995_07
Patent number
US05434150

Reaction notes

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