Cyanamide → HCID 178500509, compound

HRID 1647891Notes

Reaction equation

HRID 1647891 reaction equation
Cl.[NH2:2][C:3]1[CH:4]=[C:5]([C:9]2[N:13]([CH3:14])[C:12]3[CH:15]=[CH:16][C:17]([C:19]([NH:21][CH2:22][CH2:23][CH2:24][C:25]([O:27][CH3:28])=[O:26])=[O:20])=[CH:18][C:11]=3[N:10]=2)[CH:6]=[CH:7][CH:8]=1.[N:29]#[C:30][NH2:31]>O1CCOCC1>[NH:2]([C:3]1[CH:4]=[C:5]([C:9]2[N:13]([CH3:14])[C:12]3[CH:15]=[CH:16][C:17]([C:19]([NH:21][CH2:22][CH2:23][CH2:24][C:25]([O:27][CH3:28])=[O:26])=[O:20])=[CH:18][C:11]=3[N:10]=2)[CH:6]=[CH:7][CH:8]=1)[C:30]([NH2:31])=[NH:29]

Participants

4

Reactant 2

HCID 9864CyanamideHCID 19921247HCID 19921247, compound

Product 1

HCID 178500509HCID 178500509, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

Prepared from 2-(3-amino-phenyl)-5-[(3-methoxycarbonyl-propyl)-aminocarbonyl]-1-methyl-benzimidazole-hydrochloride by refluxing for 3 hours with cyanamide in dioxane.

Sources & evidence

ORD record
ord-706d47c8ee1d422d97b40e929311338e
Source dataset
uspto-grants-1995_07
Patent number
US05434150

Reaction notes

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