HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178485715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Maleic Anhydride | HCID 7923 | — |
| Catalyst | Cobalt | HCID 104730 | — |
| Product | 1-Methylpyrrolidine | HCID 8454 | 5% |
| Product | HCID 178485715 | HCID 178485715 | 6% |
Reaction Steps
An aqueous solution of maleic anhydride and methylamine (20 wt % of maleic anhydride/methylamine, molar ratio 1:1.5) was hydrogenated over a cobalt catalyst at 250° C. and 250 bar. Following subsequent purification, by distillation, of the hydrogenation product stream there were obtained 71% of N-methylpyrrolidone, 5% of N-methylpyrrolidine, and 6% of succinic acid-N-methylimide. There remained 17% of residue (calculated as succinic acid-N-methylamide).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05434273 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-a70d553990c4490fbdd363af883c6431 |
| Source note | uspto-grants-1995_07 |