HuagongsheHuagongshe Chemistry Print Report · For research reference only
(E)-3-[3-[[5-(Acetyloxy)pentyl]oxy]phenyl]-2-propenoic Acid Methyl Ester → 3-[[5-(Acetyloxy)pentyl]oxy]benzenepropanoic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (E)-3-[3-[[5-(Acetyloxy)pentyl]oxy]phenyl]-2-propenoic Acid Methyl Ester | HCID 67780031 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-[[5-(Acetyloxy)pentyl]oxy]benzenepropanoic acid methyl ester | HCID 54007021 | 97% |
Reaction Steps
Using the procedure of example 29, except that methanol was used as the solvent, (E)-3-[3-[[5-(acetyloxy)pentyl]oxy]phenyl]-2-propenoic acid methyl ester was hydrogenated giving 3-[[5-(acetyloxy)pentyl]oxy]benzenepropanoic acid methyl ester as a pale-yellow oil, in 97% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05434186 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-ce5014a8d4ed45b2898d1b1c3b066b30 |
| Source note | uspto-grants-1995_07 |