HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromopentyl acetate → HCID 67780195, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromopentyl acetate | HCID 85140 | — |
| Reactant | Methyl 3-(2-hydroxyphenyl)prop-2-enoate | HCID 89400 | — |
| Product | HCID 67780195 | HCID 67780195 | — |
Reaction Steps
Using the procedure of example 63, 1.78 g (10 mmol) of methyl 2-hydroxycinnamate was alkylated with 2.3 g (11 mmol) of 5-bromopentyl acetate giving (E)-3-[2-[[5-(acetyloxy)pentyl]oxy]phenyl]-2-propenoic acid methyl ester, as a pale-yellow oil, in quantitative yield. The crude product was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05434186 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-8c4fac1f412442ae893a8d36a02db11b |
| Source note | uspto-grants-1995_07 |