HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 7-bromoheptanoate → HCID 67780061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 7-bromoheptanoate | HCID 122490 | — |
| Reactant | rac-(E)-3-[2-hydroxy-6-[6-[(tetrahydro-2H-pyran-2-yl)oxy]-1-hexynyl]phenyl]-2-propenoic acid methyl ester | HCID 67694793 | — |
| Product | HCID 67780061 | HCID 67780061 | 98% |
Reaction Steps
Using the procedure of example 122, rac-(E)-3-[2-hydroxy-6-[6-[(tetrahydro-2H-pyran-2-yl)oxy]-1-hexynyl]phenyl]-2-propenoic acid methyl ester (example 121), was alkylated with ethyl 7-bromoheptanoate giving the title compound as a pale-yellow oil, in 98% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05434186 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-bc2b8e36ae41449f82c35f88c348f30e |
| Source note | uspto-grants-1995_07 |