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HRID1648153

反应详情

EQUATION

反应方程式

HRID 1648153 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)O
HCID176

Acetic Acid

C2H4O2

结构：c1ccc2c(c1)ccc1ncccc12
HCID6796

Benzo(f)quinoline

C13H9N

结构：[O-][I+2]([O-])O[I+2]([O-])[O-]
HCID159402

Iodine pentoxide (I2O5)

I2O5

PRODUCTS

生成物

1
结构：O=C1C=Cc2ccc3ncccc3c2C1=O
HCID19922456

未命名化合物

PROCEDURE

实验过程

Following the procedure described in Example 608, Part A, 37.5 g (0.153 mole) of commercial 1-azaphenanthrene, 55 g (0.165 mole) of iodine pentoxide in 600 ml glacial acetic acid were refluxed 2 hours. Identical workup yielded 8.4 g, m.p. 215°-216°.

WORKUP

后处理

  1. temperaturewere refluxed 2 hours
  2. customIdentical workup yielded 8.4 g, m.p. 215°-216°