HuagongsheHuagongshe Chemistry Print Report · For research reference only
alpha-Bromo-o-chlorotoluene → 5-Chloro-1-(2-chlorophenyl)-2-pentanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | alpha-Bromo-o-chlorotoluene | HCID 11905 | — |
| Reactant | alpha-Bromo-o-fluorotoluene | HCID 67968 | — |
| Reactant | 4-Chlorobutyryl chloride | HCID 78370 | — |
| Reactant | Cyclobutanecarbonyl chloride | HCID 78705 | — |
| Product | 5-Chloro-1-(2-chlorophenyl)-2-pentanone | HCID 19919506 | 79% |
Reaction Steps
Following a procedure similar to that described in Preparation 13, except that equivalent amounts of 2-chlorobenzyl bromide and 4-chlorobutyryl chloride were used in place of the 2-fluorobenzyl bromide and cyclobutanecarbonyl chloride, the title compound was obtained as a yellow oil in a yield of 79%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05436242 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-67f0ab57208b44999a89a24199e75eff |
| Source note | uspto-grants-1995_07 |