HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19919303, compound → HCID 19919459, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19919303 | HCID 19919303 | — |
| Solvent | Hydrogen Bromide | HCID 260 | — |
| Product | HCID 19919459 | HCID 19919459 | — |
Reaction Steps
5,6-Dihydro-7-methoxy-N,N-dipropyl-4H-imidazo(4,5,1 -ij)quinolin-5 -amine (1.0 g) was heated at 130° C. in 48% hydrobromic acid for 2 hours. The solution was cooled and was then evaporated under reduced pressure. The solid thus obtained was crystallized from methanol: ether; mp 270° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05436240 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-005af1f8010f442499f0564090b318c4 |
| Source note | uspto-grants-1995_07 |