HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19919416, compound → HCID 53876013, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19919416 | HCID 19919416 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53876013 | HCID 53876013 | 100.4% |
Reaction Steps
A mixture of 6-bromo-1,2,3,4-tetrahydro-8-nitro-N,N-dimethyl-3-quinolinamine (1.15 g, 3.8 mmol) and 10% palladium charcoal (0.5 g) in ethanol (150 mL) was hydrogenated for 18 hours. The solution was filtered and the ethanol evaporated to give 0.73 g of 1,2,3,4-tetrahydro-N3, N3 -dimethyl-3,8-quinolinediamine as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05436240 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-ce0a6da0543248fba9ea01b468db2076 |
| Source note | uspto-grants-1995_07 |