HuagongsheHuagongshe Chemistry Print Report · For research reference only
O,O-Dipyridin-2-yl carbonothioate → HCID 19919467, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O,O-Dipyridin-2-yl carbonothioate | HCID 719784 | — |
| Reactant | HCID 54046780 | HCID 54046780 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19919467 | HCID 19919467 | — |
Reaction Steps
This compound was prepared using the procedure of Example 66, but substituting chloroacetic anhydride for di (2-pyridyl)thiocarbonate and cyclizing the initially formed N8 -(chloroacetyl)-1,2,3,4-tetrahydro-N3,N3 -dimethyl-3,8-quinolinediamine by heating at 150° C. in DMF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05436240 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-e1aa09cac05b40bfb48e5d059c9ac82a |
| Source note | uspto-grants-1995_07 |