HCID 131719062, compound → HCID 54090685, compound

Participants

Reaction Steps

To a solution of Cbz-D-Phe-Pro-O-t-Bu (29 g, 64 mmol) in ethanol (500 mL) was added 5% Pd/C (14.5 g). The mixture was shaken on a hydrogenation apparatus for 16 h under 60 psi H2. The solution was then filtered through a pad of Celite® and concentrated in vacuo to give 17.5 g (86%) of thick oil.

Provenance & Evidence