HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 178475063, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 178475064 | HCID 178475064 | — |
| Product | HCID 178475063 | HCID 178475063 | — |
Reaction Steps
By methods substantially equivalent to those described in Example 51, using acetyl chloride in place of MeSO2Cl , 210 mg of Ac-D-Phe-Pro-Arg-H.HCl dihydrate was prepared. Ac-D-Phe-Pro-Arg-H.HCl was purified by RPHPLC (95/5 (A/B), 80 min; ramp to 75/25 (A/B), 320 min; hold to 360 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05436229 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-55a1f85f84344926a211af0b1578f282 |
| Source note | uspto-grants-1995_07 |