2-Aminopyridine → N'-(2-Pyridyl)-N-methyl-N-phenylformamidine

関与物質

役割	名称	HCID	仕込み量
反応物	2-Aminopyridine	HCID 10439	—
反応物	N-Methylformanilide	HCID 66737	—
生成物	N'-(2-Pyridyl)-N-methyl-N-phenylformamidine	HCID 53887703	—

反応手順

Prepared following the procedure of Example 1 from N-methylformanilide and 2-aminopyridine. Vacuum distillation of the crude product gave pure 3 as a pale yellow oil: bp 164°-165° C. @ 0.5 mm Hg. 1H-NMR (CDCl3) 8.94 (S, 1H), 8.30 (d, 1H, J=5 Hz), 7.6-6.9 (m, 8H), 3.52 (S, 3H); IR(neat) 3045, 1620, 1580, 1555, 1500, 1460, 1435, 1235; MS (m/e) 211 (M+), 106 (base).

情報源と証拠

DOI	10.6084/m9.figshare.5104873.v1
特許番号	US05436338
出典データセット	uspto-grants-1995_07
ORD ID	ord-ab2d1e9e40c54702b441d2751bd01e1e
出典メモ	uspto-grants-1995_07