HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → 1,4-Dimethyl-3,5-bis(2-chlorophenyl)-1,2,4-triazolium methylsulphate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | 1-Methyl-3,5-bis(2-chlorophenyl)-1,2,4-triazole | HCID 21463670 | — |
| Product | 1,4-Dimethyl-3,5-bis(2-chlorophenyl)-1,2,4-triazolium methylsulphate | HCID 178503011 | 189.8% |
Reaction Steps
The product of Example 1 (15.0 g) and dimethyl sulphate (6.3 g) were heated at 150° C. for 30 minutes. The melt yielded, on crystallisation from petroleum, 20.4 g of desired product, mp 135°-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04414221 |
| Source dataset | uspto-grants-1983_11 |
| ORD ID | ord-231d1059aa3b44debbe45970c0a212c2 |
| Source note | uspto-grants-1983_11 |