HuagongsheHuagongshe Chemistry Print Report · For research reference only
Caprolactam → Laurocapram
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Caprolactam | HCID 7768 | — |
| Reactant | 1-Bromododecane | HCID 8919 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Product | Laurocapram | HCID 42981 | 80.4% |
Reaction Steps
Following example 10, 15.3 g of 50% sodium hydride-mineral oil dispersion (7.65 g NaH, 0.319 M), 30 g (0.266 M) of azacycloheptan-2-one and 66.1 g (0.265 M) of 1-bromododecane on 20 hr. reflux gave 60 g (80%) of colorless product; b.p. 175°-180° /0.3 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04415563 |
| Source dataset | uspto-grants-1983_11 |
| ORD ID | ord-c805c71205df4cbcafcc9471f3244b12 |
| Source note | uspto-grants-1983_11 |