HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 15588907, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 12854869 | HCID 12854869 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15588907 | HCID 15588907 | — |
Reaction Steps
A mixture of 10.3 g. (0.036 mole) 2-(3-ethyl-5-methyl-4-isoxazolyl)-3-indole acetic acid and 22.0 g. (0.185 mole) thionyl chloride in 100 ml. toluene is stirred at room temperature for 18 hours. The toluene is removed in vacuo to give 2-(3-ethyl-5-methyl-4-isoxazolyl)-3-indole acetyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04415568 |
| Source dataset | uspto-grants-1983_11 |
| ORD ID | ord-d67e1c370d8f4336adf934e03b3e0e21 |
| Source note | uspto-grants-1983_11 |