HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13317110, compound → HCID 13317111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13317110 | HCID 13317110 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 13317111 | HCID 13317111 | 0.1% |
Reaction Steps
8-Acetylaminocarbostyril (15.0 g, 74.2 mols) was suspended in 300 ml of dioxane. After adding 2.0 g of 10% palladium-carbon, the suspension was subjected to catalytic reduction at 70° to 80° C. under atmospheric pressure. After completion of reaction, the catalyst was removed by filtration and the solvent was distilled off under reduced pressure to give 14.3 g of 8-acetylamino-3,4-dihydrocarbostyril.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04415572 |
| Source dataset | uspto-grants-1983_11 |
| ORD ID | ord-754a5691ddc048f6885fda1de4e785a1 |
| Source note | uspto-grants-1983_11 |