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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1649204Generated: November 2, 2026

HCID 13317110, compound → HCID 13317111, compound

https://huagongshe.com/reaction/1649204

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 13317110HCID 13317110—
CatalystHCID 178418390HCID 178418390—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 13317111HCID 133171110.1%

Reaction Steps

8-Acetylaminocarbostyril (15.0 g, 74.2 mols) was suspended in 300 ml of dioxane. After adding 2.0 g of 10% palladium-carbon, the suspension was subjected to catalytic reduction at 70° to 80° C. under atmospheric pressure. After completion of reaction, the catalyst was removed by filtration and the solvent was distilled off under reduced pressure to give 14.3 g of 8-acetylamino-3,4-dihydrocarbostyril.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04415572
Source datasetuspto-grants-1983_11
ORD IDord-754a5691ddc048f6885fda1de4e785a1
Source noteuspto-grants-1983_11