Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl Chloride | HCID 6327 | — |
| Reactant | Trimethyl phosphite | HCID 8472 | — |
| Reactant | 2-(4-Chlorophenoxy)-2-methylpropanoyl chloride | HCID 2781312 | — |
| Product | HCID 13841493 | HCID 13841493 | 72.1% |
Reaction Steps
An amount of 10.6 g (86 mmol) of trimethyl phosphite was added dropwise to 20.0 g (86 mmol) of p-chlorophenoxyisobutyryl chloride cooled to 0° C. As verification of the reaction, evolution of methyl chloride could be observed. Distillation under reduced pressure gave 19.0 g (62 mmol) of dimethyl p-chlorophenoxyisobutyrylphosphonate as an almost colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04416877 |
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| Source dataset | uspto-grants-1983_11 |
|---|
| ORD ID | ord-dabc7c0dbfa54c1882c74d4d9ceef6d2 |
|---|
| Source note | uspto-grants-1983_11 |
|---|
