HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthaldehyde → HCID 56617092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthaldehyde | HCID 6195 | — |
| Reactant | Ethyl 4-chloroacetoacetate | HCID 69484 | — |
| Product | HCID 56617092 | HCID 56617092 | — |
Reaction Steps
9.85 g of 1-naphthaldehyde were reacted with 15.2 g of 4-chloroacetoacetic acid ethyl ester in the course of 10 hours as described in Example 24. After incipient distillation under a high vacuum had been carried out, a 2:1 isomer mixture which still contained traces of aldehyde remained as the residue.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04416880 |
| Source dataset | uspto-grants-1983_11 |
| ORD ID | ord-5fcea39303c7496fa3b21e2f064813b6 |
| Source note | uspto-grants-1983_11 |