HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12850293, compound → HCID 12850294, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12850293 | HCID 12850293 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Hydrogen Bromide | HCID 260 | — |
| Product | HCID 12850294 | HCID 12850294 | — |
Reaction Steps
Crude ethyl 5-(bromomethyl)-1,3-diacetyl-2,3-dihydro-2-oxo-1H-imidazole-4-carboxylate is dissolved in 30% hydrobromic acid in acetic acid and the solution is allowed to stand at room temperature for 4 hours. The product precipitates, is collected and dried in vacuo at 80° C. over KOH, m.p. 193°-194° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04418071 |
| Source dataset | uspto-grants-1983_11 |
| ORD ID | ord-498165c7669640cfa19e75fb4df99099 |
| Source note | uspto-grants-1983_11 |