HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 14013762, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 14013761 | HCID 14013761 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14013762 | HCID 14013762 | 93.7% |
Reaction Steps
A mixture of 15.13 g (0.040 mol) of product of Example 27, 2.85 g (0.040 mol) of sodium azide and 175 ml of DMF was stirred for 1 hour and poured into 500 ml of water. The mixture was extracted with ether. The ether was extract was washed several times with water, dried (MgSO4) and concentrated to give 14.4 g (93.7%) of product; mp 46°-47° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04921530 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-4b8e2a49281e46338abdc2ca6e0ceea6 |
| Source note | uspto-grants-1990_05 |