HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 14013801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Dipropylamine | HCID 8902 | — |
| Reactant | HCID 14013761 | HCID 14013761 | — |
| Product | HCID 14013801 | HCID 14013801 | 96.3% |
Reaction Steps
This compound was prepared as described in Example 37: 7.0 g (0.018 mol) of product of Example 27, 5.1 ml (0.037 mol) of dipropylamine in 30 ml of DMF were reacted at room temperature affording 7.7 g (96.3%) of solid which was recrystallized in hot hexane to give 2.19 g of product as a tan solid; mp 65°-66° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04921530 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-d5978c50bc2646efb01092077b57ab6d |
| Source note | uspto-grants-1990_05 |