Trichlorosilane → HCID 131716372, compound

HRID 1650385Notes

Reaction equation

HRID 1650385 reaction equation
[CH2:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]([F:13])([F:12])[F:11])=[CH:6][C:5]=1[OH:14])[CH:2]=[CH2:3].[Cl:15][SiH:16](Cl)[Cl:17]>ClC(Cl)=C(Cl)Cl>[CH2:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]([F:12])([F:13])[F:11])=[CH:6][C:5]=1[O:14][SiH:16]([Cl:17])[Cl:15])[CH:2]=[CH2:3]

Participants

4

Reactant 2

HCID 24811TrichlorosilaneHCID 19989023HCID 19989023, compound

Product 1

HCID 131716372HCID 131716372, compound

Reagents, catalysts & solvents 1

HCID 31373TetrachloroethyleneSolvent

Procedure

607 g (3 mol) of 2-allyl-5-trifluoromethylphenol as a solution in 600 ml of perchlorethylene was reacted with 1626 g (12 mol) of trichlorosilane to form 2-allyl-5-trifluoromethylphenoxydichlorosilane. BP/1 103 to 105° C.

Sources & evidence

ORD record
ord-5b34e135f7124fa192849a6cc84aac3f
Source dataset
uspto-grants-1990_05
Patent number
US04924021

Reaction notes

Loading…