Sodium Acetate → HCID 23047120, compound

Participants

Reaction Conditions

Reaction Steps

Into a 5 liter reaction vessel is placed 820 grams of sodium acetate and 1800 grams of acetic acid. The mixture, with stirring is heated to a 100° C. While maintaining the temperature at 100° C. over a period of one hour, 1500 grams of the triisobutylene chloride prepared according to Example I is added to the reaction mass. At the end of the one hour period, the temperature is raised to 120° C. at reflux and maintained at reflux for a period of two hours. At the end of the two hour period, acetic acid is removed from the reaction mass using a Bidwell apparatus, the pot temperature being 150°-155° C. The temperature is maintained at 155° C. for a period of six hours. At the end of the six hour period, the reaction mass is cooled to 80° C. and 2 liters of water is added thereto. The reaction mass is then washed (to neutral) with sodium carbonate. The reaction mass is then distilled yielding the following fractions:

Provenance & Evidence