Sulfuryl chloride → HCID 54423660, 화합물

HRID 1650574노트

반응식

HRID 1650574 반응식
[CH2:1]([O:9][N:10]=[C:11]([C:17](=[O:19])[CH3:18])[C:12]([O:14][CH2:15][CH3:16])=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S(Cl)([Cl:23])(=O)=O>C(O)(=O)C>[CH2:1]([O:9][N:10]=[C:11]([C:17](=[O:19])[CH2:18][Cl:23])[C:12]([O:14][CH2:15][CH3:16])=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

참가 물질

4

반응물 2

HCID 24648Sulfuryl chlorideHCID 54485478HCID 54485478, 화합물

생성물 1

HCID 54423660HCID 54423660, 화합물수율 90.9%

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

Ethyl 2-n-octyloxyimino-3-oxobutyrate (syn isomer, 165.5 g.), sulfuryl chloride (84.7 g.) and acetic acid (165 ml.) were treated in a similar manner to that of Example F-(2) to give ethyl 2-n-octyloxyimino-4-chloro-3-oxobutyrate (syn isomer, 169.6 g.), oil.

출처 및 근거

ORD 기록
ord-33713080ab5946cfa5df26ffdcd65832
출처 데이터셋
uspto-grants-1990_05
특허 번호
US04923998

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