反应详情

Caprylolactam (Fluka, N.Y., #21631) (25 g, 117 mmoles), is combined with lithium aluminum hydride (10.5 g) in ether and reduced with stirring for 5 hr. The reaction mixture is filtered and evaporated with ether. The product is octahydroazonin (90% yield).

1. filtrationThe reaction mixture is filtered
2. customevaporated with ether