HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dinitrotoluene → beta-Dipropylamino-2,3-dinitrostyrene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dinitrotoluene | HCID 11761 | — |
| Reactant | 1-tert-Butoxy-N,N,N',N'-tetrapropylmethanediamine | HCID 13771313 | — |
| Product | beta-Dipropylamino-2,3-dinitrostyrene | HCID 54130656 | 85.8% |
Reaction Steps
For two hours, 5.5 g of 2,3-dinitrotoluene is heated with 13.0 g of bisdipropylamino-tert-butoxymethane to 60° C. After cooling, the reaction mixture is freed of volatile components under a high vacuum, thus obtaining 7.6 g of β-dipropylamino-2,3-dinitrostyrene as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04925854 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-beb7c777ba3f47c29ea191bf7f02fde5 |
| Source note | uspto-grants-1990_05 |