HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2,3-Dichloro-5-(trichloromethyl)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | 2-Bromo-3-chloro-5-methylpyridine | HCID 12630984 | — |
| Product | 2,3-Dichloro-5-(trichloromethyl)pyridine | HCID 94647 | — |
Reaction Steps
The product from paragraph (i) (2.9 g) in dry carbon tetrachloride (25 ml) was treated with dry hydrogen chloride to convert it to the hydrochloride. Chlorine was passed through the suspension which was kept at 80° C. and illuminated by an ultra-violet lamp inside the reaction flask. After three hours the solvent was removed, leaving a residue of 2,3-dichloro-5-trichloromethylpyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04925947 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-42e1c326480e49cbac9d9f649d374f89 |
| Source note | uspto-grants-1990_05 |