HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15617260, compound → HCID 15617261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15617260 | HCID 15617260 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 15617261 | HCID 15617261 | 80.5% |
Reaction Steps
A solution of 5.7 g of 3-bromomethyl-2-carboethoxy-N-(1,1-dimethylethyl)benzenesulfonamide in 60 mL of trifluoroacetic acid was stirred at room temperature for 16 hours. Concentration provided a viscous oil which was triturated with n-butyl chloride. The solids were collected to yield 3.91 g of a white solid, m.p. 138°-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04927453 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-b7ee9caf142d4d718e8e0cfba5a73046 |
| Source note | uspto-grants-1990_05 |