HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → HCID 15097581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 15097580 | HCID 15097580 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 15097581 | HCID 15097581 | 92.1% |
Reaction Steps
7-Methoxy-1-(3-methoxyphenyl)-2-naphthalenemethanol (1.75 g) was oxidized using the reagent prepared as in Example 136 from oxalyl chloride (0.62 mL) and dimethylsulfoxide (0.9 mL) in dichloromethane (14 mL). The usual work up furnished 1.6 g of 7-methoxy-1-(3-methoxyphenyl)-2-naphthalenecarboxaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04927838 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-68759b11c0fc4f31b774932232fdfcd1 |
| Source note | uspto-grants-1990_05 |