HCID 13773263, compound → 1,3,4-Thiadiazole-2-carboxylic acid, 3-[6-amino-2-[(1-carboxy-3-phenylpropyl)amino]-1-oxohexyl]-5-(1,1-dimethylethyl)-2,3-dihydro-, [2S-[2R*,3[R*(R*)]]]-

Participants

Reaction Steps

A solution of the product from step d) (1.lg) in ethanol (90ml) was treated with 10% palladium on carbon (0.9g) and the mixture stirred under 1 atmosphere of hydrogen for 1 hour. The catalyst was removed by filtration and the filtrate evaporated. The residue was recrystallised from a mixture of tetrahydrofuran and ethanol to give the title product as a white solid (0.24g)

Provenance & Evidence