Hydrogen Sulfide → HCID 13773280, compound

HRID 1651450Notes

Reaction equation

HRID 1651450 reaction equation
[SH2:1].C(OC([C@@H](N[C@H](C(N1N=[C:24]([C:26]2[CH:31]=[CH:30][C:29]([S:32][CH3:33])=[CH:28][CH:27]=2)[S:23][C@H:22]1[C:34]([OH:36])=[O:35])=O)C)CCC1C=CC=CC=1)=O)C>CO>[CH3:33][S:32][C:29]1[CH:30]=[CH:31][C:26]([C:24](=[S:1])[S:23][CH2:22][C:34]([OH:36])=[O:35])=[CH:27][CH:28]=1

Participants

4

Reactant 2

HCID 402Hydrogen SulfideHCID 13773286HCID 13773286, compound

Product 1

HCID 13773280HCID 13773280, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Hydrogen sulphide was passed through a solution of the product of step (b) (25.0g) in methanol (250ml) and cooled in an ice bath, for a period of 3 hours.

Workup

  1. temperaturecooled in an ice bath, for a period of 3 hours

Sources & evidence

ORD record
ord-e8ee4e4cf0ef4316b72a5a20d409e6c0
Source dataset
uspto-grants-1990_05
Patent number
US04927822

Reaction notes

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