3-(Acetylsulfanyl)propanoyl chloride → HCID 13773323, compound

HRID 1651466Notes

Reaction equation

HRID 1651466 reaction equation
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[C:11]1[S:15][CH:14]([C:16]([O:18][CH2:19][CH3:20])=[O:17])[NH:13][N:12]=1.[C:21]([S:24][CH2:25][CH2:26][C:27](Cl)=[O:28])(=[O:23])[CH3:22]>>[C:21]([S:24][CH2:25][CH2:26][C:27]([N:13]1[N:12]=[C:11]([C:2]2[CH:3]=[CH:4][C:5]3[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=3)[CH:1]=2)[S:15][CH:14]1[C:16]([O:18][CH2:19][CH3:20])=[O:17])=[O:28])(=[O:23])[CH3:22]

Participants

3

Reactant 2

HCID 129431223-(Acetylsulfanyl)propanoyl chlorideHCID 13773322HCID 13773322, compound

Product 1

HCID 13773323HCID 13773323, compound

Procedure

Prepared from the crude product of step (b) and 3-acetylthiopropanoyl chloride by the process of Example 3, step (b). mp 107°-108°

Sources & evidence

ORD record
ord-a442f909eecc40889228293d3f6f691e
Source dataset
uspto-grants-1990_05
Patent number
US04927822

Reaction notes

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