3-(Acetylsulfanyl)propanoyl chloride → HCID 23051217, compound

HRID 1651469Notes

Reaction equation

HRID 1651469 reaction equation
[C:1]12([C:11]3[S:15][CH:14]([C:16]([O:18][CH2:19][CH3:20])=[O:17])[NH:13][N:12]=3)[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.C([S:24][CH2:25][CH2:26][C:27](Cl)=[O:28])(=O)C>>[C:1]12([C:11]3[S:15][CH:14]([C:16]([O:18][CH2:19][CH3:20])=[O:17])[N:13]([C:27](=[O:28])[CH2:26][CH2:25][SH:24])[N:12]=3)[CH2:8][CH:7]3[CH2:9][CH:3]([CH2:4][CH:5]([CH2:6]3)[CH2:10]1)[CH2:2]2

Participants

3

Reactant 2

HCID 129431223-(Acetylsulfanyl)propanoyl chlorideHCID 23051223HCID 23051223, compound

Product 1

HCID 23051217HCID 23051217, compound

Procedure

The crude product of step (c) was treated with 3-acetylthiopropanoyl chloride by the process of Example 3, step (b) to give the sub-title product as an oil.

Sources & evidence

ORD record
ord-691d8174f6b34310b5cac0afd6ee79c9
Source dataset
uspto-grants-1990_05
Patent number
US04927822

Reaction notes

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