Potassium Hydroxide → HCID 13773327, compound

HRID 1651470Notes

Reaction equation

HRID 1651470 reaction equation
[C:1]12([C:11]3[S:15][CH:14]([C:16]([O:18]CC)=[O:17])[N:13]([C:21](=[O:25])[CH2:22][CH2:23][SH:24])[N:12]=3)[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[OH-].[K+]>>[C:1]12([C:11]3[S:15][CH:14]([C:16]([OH:18])=[O:17])[N:13]([C:21](=[O:25])[CH2:22][CH2:23][SH:24])[N:12]=3)[CH2:8][CH:7]3[CH2:9][CH:3]([CH2:4][CH:5]([CH2:6]3)[CH2:10]1)[CH2:2]2

Participants

3

Reactant 2

HCID 14797Potassium HydroxideHCID 23051217HCID 23051217, compound

Product 1

HCID 13773327HCID 13773327, compound

Procedure

The product of step (d) was treated with potassium hydroxide by the process of Example 3, step (c) to give the title product as white solid. mp 183°-184°. Mass spectrum (FAB) showed M+ 355 (base peak 221). C16H22N2O3S2 requires MWt 354.

Sources & evidence

ORD record
ord-4769275f7dc24ef291122c37170e656a
Source dataset
uspto-grants-1990_05
Patent number
US04927822

Reaction notes

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