Titanium Tetrachloride → HCID 86698323, compound

HRID 1651496Notes

Reaction equation

HRID 1651496 reaction equation
[Al+3:1].[Cl-:2].[Cl-].[Cl-].[Cl:5][Ti:6]([Cl:9])([Cl:8])[Cl:7]>O>[Al+3:1].[Cl-:5].[Cl-:2].[Cl-:5].[Cl:5][Ti:6]([Cl:9])([Cl:8])[Cl:7]

Participants

4

Reactant 2

HCID 24193Titanium Tetrachloride3×HCID 6451240Aluminum(III) Chloride2×

Product 1

HCID 86698323HCID 86698323, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

An acidic solution is made by diluting 25 liters of a 28 weight percent (wt. %) AlCl3 solution to 60 liters total volume with water. In addition, a TiCl4 solution is made by slowly adding 800 ml of TiCl4 to 2000 ml of water to obtain a clear solution. The TiCl4 solution is then added to the AlCl3 solution to form an AlCl3 -TiCl4 solution. A base solution is made by dissolving 9,000 g of NaOH in 60 liters of water. Then the following controlled precipitation method is carried out:

Workup

  1. customto obtain a clear solution

Sources & evidence

ORD record
ord-ce4aa5a4c9524d6e9d08e8e562d3392f
Source dataset
uspto-grants-1990_05
Patent number
US04929381

Reaction notes

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