Glyoxal → HCID 15099955, compound

HRID 1651505Notes

Reaction equation

[CH2:1]([PH2:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH:10]([CH:12]=[O:13])=[O:11]>>[CH2:1]([P:9]1[CH:10]([OH:11])[CH:12]([OH:13])[P:9]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])[CH:10]([OH:11])[CH:12]1[OH:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

Reactant 2

HCID 7860Glyoxal

HCID 446269Phosphine, octyl-

Product 1

HCID 15099955HCID 15099955, compound

Procedure

Following the procedure of Example 1, 200 parts of mono-n-octylphosphine is reacted with 194 parts of glyoxal to give 1,4-di-n-octyl-2,3,5,6-tetrahydroxy-1,4-diphosphorinane, a waxy solid.

Sources & evidence

ORD record: ord-f23b6b2479b1452193a6b8b2f7fcf75f
Source dataset: uspto-grants-1990_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04929393

Reaction notes

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