HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → HCID 178471865, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | HCID 53647345 | HCID 53647345 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 178471865 | HCID 178471865 | — |
Reaction Steps
A solution of 4.50 g (11.06 mmol) of ethyl 4-(1-acetyl-1,2,3,6-tetrahydro-4-pyridyl)-α-(ethoxymethylene)-2,5-difluoro-β-oxobenzenepropionate in 50 ml of ethyl ether was treated with 0.77 g (13.5 mmol) of cyclopropylamine and stirred for 22 hours. The title compound was isolated as a syrup after evaporation under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04929613 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-5063f5a828cb43ebbf225eac3bb734f3 |
| Source note | uspto-grants-1990_05 |