HCID 23050238, compound → HCID 178486609, compound
Reaction equation
COC1C(OC)=CC2SC(/C=C/C#N)=CC=2C=1.[ClH:18].[OH:19][NH:20][C:21](=[NH:37])/[CH:22]=[CH:23]/[C:24]1[S:28][C:27]2[CH:29]=[C:30]([O:35][CH3:36])[C:31]([O:33][CH3:34])=[CH:32][C:26]=2[CH:25]=1>>[ClH:18].[OH:19][NH:20][C:21](=[NH:37])[CH:22]=[CH:23][C:24]1[S:28][C:27]2[CH:29]=[C:30]([O:35][CH3:36])[C:31]([O:33][CH3:34])=[CH:32][C:26]=2[CH:25]=1Participants
3
Procedure
Using the procedure described in Example 2 (E)-3-(5,6-dimethoxy-benzo[b]thiophene-2-yl)-2-propenenitrile was converted into (E)-N-hydroxy-3-(5,6-dimethoxy-benzo[b]thiophene-2-yl)-prop-2-eneimidamide hydrochloride, m.p. 188°-198° C. (decomp.).
Sources & evidence
- ORD record
- ord-f9cff82d38184125959c0e210f1a69b8
- Source dataset
- uspto-grants-1990_05
- Patent number
- US04929636
Reaction notes
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