HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → 1,1-Diphenylethane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Catalyst | Iron | HCID 23925 | — |
| Catalyst | Cuprous chloride | HCID 62652 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1,1-Diphenylethane | HCID 11918 | 71.4% |
Reaction Steps
The procedure of Example I was repeated except that the reaction mass contained 150 ml water, 5.6 g iron (99.9+% pure), 0.2 g CuCl (99.9% pure), and 25.4 g benzyl chloride. The reaction period was for 3 hr. 13.0 g of crude diphenylethane product was obtained. This represents a 71.4% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04929785 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-71e142610d554d66ac361faaf2269a06 |
| Source note | uspto-grants-1990_05 |