HCID 54065807, compound → HCID 53919116, compound

HRID 1651876Notes

Reaction equation

HRID 1651876 reaction equation
[C:1]1([CH3:26])[CH:6]=[CH:5][C:4]([S:7]([NH:10][CH:11]2[CH2:19][C:18]3[C:13](=[CH:14][CH:15]=[C:16]([CH:20]([CH3:25])[C:21]([O:23]C)=[O:22])[CH:17]=3)[CH2:12]2)(=[O:9])=[O:8])=[CH:3][CH:2]=1>C(O)C>[C:1]1([CH3:26])[CH:2]=[CH:3][C:4]([S:7]([NH:10][CH:11]2[CH2:19][C:18]3[C:13](=[CH:14][CH:15]=[C:16]([CH:20]([CH3:25])[C:21]([OH:23])=[O:22])[CH:17]=3)[CH2:12]2)(=[O:8])=[O:9])=[CH:5][CH:6]=1

Participants

3

Reactant 1

HCID 54065807HCID 54065807, compound

Product 1

HCID 53919116HCID 53919116, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

1 ml of 15N sodium hydroxide solution is added to 1.2 g of methyl 2-(2-p-toluenesulphonamido-indan-5-yl)-propionate in 12 ml of ethanol and the mixture is boiled for 0.5 hour. The mixture is evaporated, the residue is dissolved in water and the reaction product is precipitated with hydrochloric acid.

Workup

  1. customThe mixture is evaporated
  2. dissolutionthe residue is dissolved in water
  3. customthe reaction product is precipitated with hydrochloric acid

Sources & evidence

ORD record
ord-390515b174f7499c94d772204acad028
Source dataset
uspto-grants-1990_05
Patent number
US04929754

Reaction notes

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