HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1653935Generated: October 30, 2026
(3-(Trifluoromethyl)phenyl)hydrazine → Sophorose
https://huagongshe.com/reaction/1653935
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | (3-(Trifluoromethyl)phenyl)hydrazine | HCID 98650 | — |
| Reactant | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | D-glucose 3-(trifluoromethyl)phenyl hydrazone | HCID 86748606 | — |
| Solvent | Water | HCID 962 | — |
| Product | Sophorose | HCID 92797 | — |
Reaction Steps
To this oligosaccharide (10 μmol), sodium acetate (30 μmol) in a small vial (Pierce reacti-vial, 0.2 mL capacity, with Tuf-bond Teflon-silicone cap seals) was added 150 μL water. 3-(trifluoromethyl)phenylhydrazine (40 μmol, Aldrich) was added, the sample sealed under nitrogen, and heated to 90° C. for 48 hours. The oligosaccharide was converted (>98%) to D-glucose and D-glucose 3-(trifluoromethyl)phenyl hydrazone, in a 1:2 ratio.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05403927 |
|---|
| Source dataset | uspto-grants-1995_04 |
|---|
| ORD ID | ord-497474b42c1c45b88ea6d1649eb81a59 |
|---|
| Source note | uspto-grants-1995_04 |
|---|