1-(3-Hydroxypropyl)-5,6-dimethylbenzimidazole → HCID 20078959, compound

HRID 1653994Notes

Reaction equation

HRID 1653994 reaction equation
OCCC[N:5]1[C:9]2[CH:10]=[C:11]([CH3:15])[C:12]([CH3:14])=[CH:13][C:8]=2[N:7]=[CH:6]1.[NH+]1C=CC=CC=1.[C:22]([CH2:24][CH2:25][O:26][P:27](=[O:30])([O-:29])[O-:28])#N.[NH+]1C=CC=CC=1>>[CH3:15][C:11]1[C:12]([CH3:14])=[CH:13][C:8]2[N:7]=[C:6]([CH2:22][CH2:24][CH2:25][O:26][P:27](=[O:28])([OH:30])[OH:29])[NH:5][C:9]=2[CH:10]=1

Participants

3

Reactant 2

HCID 200789601-(3-Hydroxypropyl)-5,6-dimethylbenzimidazoleHCID 69780213Pyridinium cyanoethylphosphate

Product 1

HCID 20078959HCID 20078959, compound

Procedure

Using 0.2 g of the crude 1-(3-hydroxypropyl)-5,6-dimethylbenzimidazole and 2 ml of 2-cyanoethylphosphoric acid pyridinium salt solution (1 mmol/ml) as the starting substances, according to the same processes as in Example 1, 0.3 g of crude 3-(5,6-dimethylbenzimidazolyl)propylphosphoric acid was obtained.

Sources & evidence

ORD record
ord-7b8e8cbc94a74b07b5252f9d064728d6
Source dataset
uspto-grants-1995_04
Patent number
US05405839

Reaction notes

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