HCID 20078963, compound → HCID 20078964, compound

HRID 1653998Notes

Reaction equation

OCCCCCC[N:8]1[C:12]2[CH:13]=[C:14]([CH3:18])[C:15]([CH3:17])=[CH:16][C:11]=2[N:10]=[CH:9]1.[NH+]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1.C(C[CH2:28][O:29][P:30](=[O:33])([O-:32])[O-:31])#N.[NH+]1C=CC=CC=1>>[CH3:18][C:14]1[C:15]([CH3:17])=[CH:16][C:11]2[N:10]=[C:9]([CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:28][O:29][P:30](=[O:31])([OH:33])[OH:32])[NH:8][C:12]=2[CH:13]=1

Participants

Reactant 2

HCID 20078963HCID 20078963, compound

HCID 69780213Pyridinium cyanoethylphosphate

Product 1

HCID 20078964HCID 20078964, compound

Procedure

Using 0.2 g of the crude 1-(6-hydroxyhexyl)-5,6-dimethylbenzimidazole and 2 ml of a 2-cyanoethylphosphoric acid pyridinium salt solution (1 mmol/ml), and subsequently following the same procedures as in Example 1, 0.35 g of crude 6-(5,6-dimethylbenzimidazolyl)hexylphosphoric acid was obtained.

Sources & evidence

ORD record: ord-4b71b992e1f54245a6dd2ea3cfd8a5cb
Source dataset: uspto-grants-1995_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05405839

Reaction notes

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