3-(1H-imidazol-1-yl)propan-1-ol → 3-Imidazolylpropylphosphoric acid

HRID 1654000Notes

Reaction equation

HRID 1654000 reaction equation
OCCC[N:5]1[CH:9]=[CH:8][N:7]=[CH:6]1.[NH+]1C=CC=CC=1.[C:16]([CH2:18][CH2:19][O:20][P:21](=[O:24])([OH:23])[OH:22])#N>>[NH:7]1[CH:8]=[CH:9][N:5]=[C:6]1[CH2:16][CH2:18][CH2:19][O:20][P:21](=[O:22])([OH:24])[OH:23]

Participants

3

Reactant 2

HCID 47122713-(1H-imidazol-1-yl)propan-1-olHCID 867486072-Cyanoethylphosphoric acid pyridinium

Product 1

HCID 200789583-Imidazolylpropylphosphoric acid

Procedure

Using 0.13 g of the purified 1-(3-hydroxypropyl)imidazole and 2 ml of 2-cyanoethylphosphoric acid pyridinium solution (1 mmol/ml), and subsequently following the same processes as in Example 1, 0.2 g of crude 3-imidazolylpropylphosphoric acid was obtained.

Sources & evidence

ORD record
ord-d11b00f9c8c94d1eb89ac8602643f0e0
Source dataset
uspto-grants-1995_04
Patent number
US05405839

Reaction notes

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