HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Nitrofurfural → HCID 20079666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Nitrofurfural | HCID 12774 | — |
| Reactant | HCID 178418486 | HCID 178418486 | — |
| Product | HCID 20079666 | HCID 20079666 | — |
Reaction Steps
Using the procedure of Stage B of Preparation 2, 2.82 g of 5-nitro-2-furaldehyde and 45 ml of ethynylmagnesium bromide were reacted to obtain 1.84 g of the expected product after chromatography on silica (eluent: 8/2 hexane/ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05405865 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-b41b8e6d05c24befbfdda6b7660caaa4 |
| Source note | uspto-grants-1995_04 |