HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromobenzonitrile → 5-(2-Bromophenyl)-1-(trimethylstannyl)-1H-tetrazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromobenzonitrile | HCID 16272 | — |
| Reactant | Azido(trimethyl)stannane | HCID 5104973 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 5-(2-Bromophenyl)-1-(trimethylstannyl)-1H-tetrazole | HCID 20079345 | — |
Reaction Steps
To a solution of 1.50 g of o-bromobenzonitrile in 8.0 ml of toluene is added 1.70 g of trimethyltin azide. The reaction mixture is heated to reflux for 18 hours and then allowed to cool to room temperature. The resulting white precipitate is isolated by filtration and used without purification in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05405849 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-6d63f93e9aec41b29a3be8645843ea71 |
| Source note | uspto-grants-1995_04 |