Sodium Bicarbonate → HCID 10668837, compound

Participants

Reaction Steps

According to Procedure B (Example 17, Step IV), a stirred mixture of N-[4-[4-(ethylamino)-1-hydroxybutyl]phenyl]methanesulfonamide (Example 7, Step II) and sodium bicarbonate in acetonitrile was allowed to react with 1-bromo-5-fluoro-5-methylhexane (Step III) to give the titled product, a compound of Formula I'. The high resolution mass spectrum had M+ at m/z 402. Theory for C20H35FN2O3S: 402.2352; measured: 402.2350.

Provenance & Evidence