Putrescine → HCID 11740258, compound

HRID 1654494Notes

Reaction equation

C([O:3][C:4]([C:6]1[C:22]2[C:10](=[C:11]([CH3:25])[C:12]3[N:13]([CH3:24])[C:14]4[CH:15]=[CH:16][C:17]([OH:23])=[CH:18][C:19]=4[C:20]=3[CH:21]=2)[CH:9]=[CH:8][N:7]=1)=O)C.[NH2:26][CH2:27][CH2:28][CH2:29][CH2:30][NH2:31]>>[NH2:26][CH2:27][CH2:28][CH2:29][CH2:30][NH:31][C:4]([C:6]1[C:22]2[C:10](=[C:11]([CH3:25])[C:12]3[N:13]([CH3:24])[C:14]4[CH:15]=[CH:16][C:17]([OH:23])=[CH:18][C:19]=4[C:20]=3[CH:21]=2)[CH:9]=[CH:8][N:7]=1)=[O:3]

Participants

Reactant 2

HCID 1045Putrescine

HCID 10246273HCID 10246273, compound

Product 1

HCID 11740258HCID 11740258, compound

Procedure

0.47 g (1.407 mmol) of the ester obtained in Step A of Example 11 are dissolved in 9 ml of 1,4-diaminobutane under an argon atmosphere. The mixture is heated at 130° for 3 hours.

Workup

temperatureThe mixture is heated at 130° for 3 hours

Sources & evidence

ORD record: ord-2a0c4eccfd9e4176924f213c37fce2ff
Source dataset: uspto-grants-1995_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05407940

Reaction notes

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